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Le prcipit ainsi form est filtr, sch sous vide (1 mmHg) pendant 24 h puis purifi par sublimation pour fournir 30 g (91%) d'un solide blanc.In a 1-liter flask equipped with a condenser and a magnetized bar, 1,4-bis (trifluoromethyl) benzene (19 g, 88.7 mmol, ABCR), trifluoroacetic acid ( 250 L, SDS) and 99% sulfuric acid (60 mL, Acros)

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